HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 13450726, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Chloroacetyl chloride | HCID 6577 | — |
| Reactant | Ammonium Carbonate | HCID 517111 | — |
| Reactant | HCID 13450696 | HCID 13450696 | — |
| Product | HCID 13450726 | HCID 13450726 | — |
Reaction Steps
The reactions are performed as in the method of Example 23 (d) and (e). Thus ethyl 4-(2-benzoylanilino)piperidine-1-carboxylate (2.56 g) is reacted successively with 2-chloro-acetyl chloride, sodium iodide and ammonium carbonate, whereby 1,3-dihydro-1-(1-ethoxycarbonyl-4-piperidinyl)-5-phenyl-2H-1,4-benzodiazepin-2-one (2.27 g) is obtained as a powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04560684 |
| Source dataset | uspto-grants-1985_12 |
| ORD ID | ord-380c7b50a20c445c8e04908eaed0530d |
| Source note | uspto-grants-1985_12 |