HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Chloromethyl)-4-methoxy-3,5-dimethylpyridine → HCID 20253699, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Chloromethyl)-4-methoxy-3,5-dimethylpyridine | HCID 819992 | — |
| Reactant | HCID 178506005 | HCID 178506005 | — |
| Product | HCID 20253699 | HCID 20253699 | 86% |
Reaction Steps
Analogous reaction of 2,2-difluoro-5H-[1,3]-dioxolo[4,5-f]benzimidazole-6-thiol with 2-chloromethyl-4-methoxy-3,5-dimethylpyridine gives 2,2-difluoro-6-[(4-methoxy-3,5-dimethyl-2-pyridyl)methylthio]-5H-[1,3]-dioxolo[4,5-f]benzimidazole, of m.p. 148°-149° C. (from acetonitrile), in 86% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04560693 |
| Source dataset | uspto-grants-1985_12 |
| ORD ID | ord-13dbcb07454c4803b58728f37b0893c4 |
| Source note | uspto-grants-1985_12 |