HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 13603935, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Ethyl 4-piperidinecarboxylate | HCID 70770 | — |
| Reactant | 4-Chloro-6-fluoro-2-phenylquinoline | HCID 13603896 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 13603935 | HCID 13603935 | — |
Reaction Steps
A mixture of 9.0 g of 4-chloro-6-fluoro-2-phenylquinoline prepared according to the procedure described in example 9(b) and 18 ml of ethyl isonipecotate was stirred and heated in an oil bath at 160°-165° for 2 hr. It was then cooled and diluted with water. Addition of ethanol caused a solid to form which was collected to give 7.2 g of product as white prisms, mp 120°-124°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04560692 |
| Source dataset | uspto-grants-1985_12 |
| ORD ID | ord-0349178e721048998d54e8bf1c3c74e6 |
| Source note | uspto-grants-1985_12 |