HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 22826632, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 22826622 | HCID 22826622 | — |
| Solvent | Formic Acid | HCID 284 | — |
| Product | HCID 22826632 | HCID 22826632 | — |
Reaction Steps
A solution of 1 g (2.44 mmol) of (±)-1-[5-amino-2-[hydroxy-(4-phenylbutyl)phosphinyl]-1-oxopentyl]-L-proline (prepared as described in Example 1) in a mixture of 5 ml of acetic anhydride and 15 ml of 90% formic acid is kept at room temperature for 3 hours, then evaporated to give the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04560680 |
| Source dataset | uspto-grants-1985_12 |
| ORD ID | ord-df2c90add6274d039ef6c9073da112ae |
| Source note | uspto-grants-1985_12 |