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HRID638391

反应详情

EQUATION

反应方程式

HRID 638391 的结构方程式

REACTANTS

反应物

3
结构：[Cl][Sn]([Cl])([Cl])[Cl]
HCID24287

Tetrachlorostannane

Cl4Sn

结构：Cl[Si](Cl)(Cl)Cl
HCID24816

Silane, tetrachloro-

Cl4Si

结构：C=CCCCCCCCCOC(C)=O
HCID39801

9-Decenyl acetate

C12H22O2

PRODUCTS

生成物

1
结构：CC(=O)OCCCCCCCCC=CCCCCCCCCOC(C)=O
HCID54538787

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Clc1ccccc1
溶剂HCID7964

Chlorobenzene

C6H5Cl

PROCEDURE

实验过程

The 300 mL autoclave was charged with 9-decenyl acetate (0.22 mol), (phenylmethoxycarbene)pentacarbonyltungsten(O) (0.001 mol), SnCl4 (0.01 mol), SiCl4 (0.02 mol) and 20 mL chlorobenzene. The autoclave was heated to 86° for 4 hours with continuous venting above 5 psig.

WORKUP

后处理

  1. temperatureThe autoclave was heated to 86° for 4 hours with continuous venting above 5 psig