Methanol → HCID 70450173, compound

Participants

Reaction Steps

14.7 g of dimethyl 3,4-dichlorophenylhydroxymalonate were dissolved in 100 ml of methanol, and methylamine was passed in for 1 hour at 60° C. The mixture was evaporated down completely and the crystalline residue was recrystallized from 100 ml of ethanol. 12 g of 3,4-dichlorophenylhydroxymalonic acid dimethylamide (m.p.=158°-60° C.) were obtained.

Provenance & Evidence