Aluminium lithium hydride → HCID 68712490, compound

Participants

Reaction Steps

A solution of 1-(3,4-Dichloro-benzyl)-azetidine-3-carbonitrile (0.083 g, 0.347 mmol) in dry THF (2 ml) cooled to 0° C. is treated with a 1.0 M solution of lithium aluminium hydride in THF (0.347 ml). The reaction mixture is allowed to warm to ambient temperature and stirred for a one hour. The reaction mixture is quenched with saturated sodium sulphate solution and filtered. The filtrate is evaporated to afford the title compound. [MH] 244.97.

Provenance & Evidence