HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 3-(hex-3-en-1-yl)-4,5-dimethoxybenzoate → Methyl 3-hexyl-4,5-dimethoxybenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 3-(hex-3-en-1-yl)-4,5-dimethoxybenzoate | HCID 68684188 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Methyl 3-hexyl-4,5-dimethoxybenzoate | HCID 68685356 | — |
Reaction Steps
3-Hexyl-4,5-dimethoxybenzoic acid methyl ester was prepared from 3-hex-3-enyl-4,5-dimethoxybenzoic acid methyl ester by following Method H using EtOAc as a solvent. The reaction was conducted for 2.5 h under hydrogen atmosphere. The product obtained in quantitative yield was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07691843B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-d6e16dcf34144d11a431166a278f78a2 |
| Source note | uspto-grants-2010_04 |