Methyl 3-(hex-3-en-1-yl)-4,5-dimethoxybenzoate → Methyl 3-hexyl-4,5-dimethoxybenzoate

HRID 638920Notes

Reaction equation

HRID 638920 reaction equation
[CH3:1][O:2][C:3](=[O:20])[C:4]1[CH:9]=[C:8]([O:10][CH3:11])[C:7]([O:12][CH3:13])=[C:6]([CH2:14][CH2:15][CH:16]=[CH:17][CH2:18][CH3:19])[CH:5]=1>CCOC(C)=O>[CH3:1][O:2][C:3](=[O:20])[C:4]1[CH:9]=[C:8]([O:10][CH3:11])[C:7]([O:12][CH3:13])=[C:6]([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19])[CH:5]=1

Participants

3

Reactant 1

HCID 68684188Methyl 3-(hex-3-en-1-yl)-4,5-dimethoxybenzoate

Product 1

HCID 68685356Methyl 3-hexyl-4,5-dimethoxybenzoate

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

3-Hexyl-4,5-dimethoxybenzoic acid methyl ester was prepared from 3-hex-3-enyl-4,5-dimethoxybenzoic acid methyl ester by following Method H using EtOAc as a solvent. The reaction was conducted for 2.5 h under hydrogen atmosphere. The product obtained in quantitative yield was used without further purification.

Workup

  1. customThe product obtained in quantitative yield
  2. customwas used without further purification

Sources & evidence

ORD record
ord-d6e16dcf34144d11a431166a278f78a2
Source dataset
uspto-grants-2010_04
Patent number
US07691843B2

Reaction notes

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