HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 3,4-dimethoxy-5-(pent-3-en-1-yl)benzoate → Methyl 3,4-dimethoxy-5-pentylbenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 3,4-dimethoxy-5-(pent-3-en-1-yl)benzoate | HCID 68682459 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Methyl 3,4-dimethoxy-5-pentylbenzoate | HCID 68685427 | — |
Reaction Steps
3,4-Dimethoxy-5-pentylbenzoic acid methyl ester was prepared 3,4-dimethoxy-5-pent-3-enylbenzoic methyl ester by following Method H using EtOAc as a solvent. The reaction was conducted for 2.5 h under hydrogen atmosphere. The product, obtained in quantitative yield, was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07691843B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-f43dd26c80b349c5907b3fa0f83b87bc |
| Source note | uspto-grants-2010_04 |