Methyl 3,4-dimethoxy-5-(pent-3-en-1-yl)benzoate → Methyl 3,4-dimethoxy-5-pentylbenzoate

HRID 638921Notes

Reaction equation

HRID 638921 reaction equation
[CH3:1][O:2][C:3](=[O:19])[C:4]1[CH:9]=[C:8]([CH2:10][CH2:11][CH:12]=[CH:13][CH3:14])[C:7]([O:15][CH3:16])=[C:6]([O:17][CH3:18])[CH:5]=1>CCOC(C)=O>[CH3:1][O:2][C:3](=[O:19])[C:4]1[CH:9]=[C:8]([CH2:10][CH2:11][CH2:12][CH2:13][CH3:14])[C:7]([O:15][CH3:16])=[C:6]([O:17][CH3:18])[CH:5]=1

Participants

3

Reactant 1

HCID 68682459Methyl 3,4-dimethoxy-5-(pent-3-en-1-yl)benzoate

Product 1

HCID 68685427Methyl 3,4-dimethoxy-5-pentylbenzoate

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

3,4-Dimethoxy-5-pentylbenzoic acid methyl ester was prepared 3,4-dimethoxy-5-pent-3-enylbenzoic methyl ester by following Method H using EtOAc as a solvent. The reaction was conducted for 2.5 h under hydrogen atmosphere. The product, obtained in quantitative yield, was used without further purification.

Workup

  1. customThe product, obtained in quantitative yield
  2. customwas used without further purification

Sources & evidence

ORD record
ord-f43dd26c80b349c5907b3fa0f83b87bc
Source dataset
uspto-grants-2010_04
Patent number
US07691843B2

Reaction notes

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