HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 8707145, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | methyl 3-allyl-4-hydroxy-5-methoxybenzoate | HCID 7131942 | — |
| Product | HCID 8707145 | HCID 8707145 | — |
Reaction Steps
3-Allyl-4-hydroxy-5-methoxybenzoic acid was prepared from 3-allyl-4-hydroxy-5-methoxybenzoic acid methyl ester (Example 1, Step 2) using Method E. In this method LiOH was replaced with NaOH and the reaction was conducted at room temperature for 18 h. The product was extracted with ether. The crude product was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07691843B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-25a07bdc8da84e82a7e195e6e048c673 |
| Source note | uspto-grants-2010_04 |