Lithium Hydroxide → HCID 8707145, compound

HRID 638922Notes

Reaction equation

HRID 638922 reaction equation
C[O:2][C:3](=[O:16])[C:4]1[CH:9]=[C:8]([O:10][CH3:11])[C:7]([OH:12])=[C:6]([CH2:13][CH:14]=[CH2:15])[CH:5]=1.[Li+].[OH-].[OH-].[Na+]>>[CH2:13]([C:6]1[CH:5]=[C:4]([CH:9]=[C:8]([O:10][CH3:11])[C:7]=1[OH:12])[C:3]([OH:16])=[O:2])[CH:14]=[CH2:15]

Participants

4

Reactant 3

HCID 3939Lithium HydroxideHCID 14798Sodium HydroxideHCID 7131942methyl 3-allyl-4-hydroxy-5-methoxybenzoate

Product 1

HCID 8707145HCID 8707145, compound

Procedure

3-Allyl-4-hydroxy-5-methoxybenzoic acid was prepared from 3-allyl-4-hydroxy-5-methoxybenzoic acid methyl ester (Example 1, Step 2) using Method E. In this method LiOH was replaced with NaOH and the reaction was conducted at room temperature for 18 h. The product was extracted with ether. The crude product was used without further purification.

Workup

  1. extractionThe product was extracted with ether
  2. customThe crude product was used without further purification

Sources & evidence

ORD record
ord-25a07bdc8da84e82a7e195e6e048c673
Source dataset
uspto-grants-2010_04
Patent number
US07691843B2

Reaction notes

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