HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 3,4-Dimethoxy-5-(3-methoxypropyl)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 3-(3-Hydroxypropyl)-4,5-dimethoxybenzoic acid | HCID 68685149 | — |
| Product | 3,4-Dimethoxy-5-(3-methoxypropyl)benzoic acid | HCID 68685215 | 69% |
Reaction Steps
3,4-Dimethoxy-5-(3-methoxypropyl)benzoic acid was prepared from 3-(3-hydroxypropyl)-4,5-Dimethoxybenzoic acid (Example 10, Step 1) and methyl iodide by following Method I in 69% yield. The product was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07691843B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-d776a3b544fa46b7a1e597b665a71539 |
| Source note | uspto-grants-2010_04 |