HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 68683485, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | methyl 3-allyl-4-hydroxy-5-methoxybenzoate | HCID 7131942 | — |
| Product | HCID 68683485 | HCID 68683485 | 96% |
Reaction Steps
3-Allyl-4,5-dimethoxybenzoic acid methyl ester was prepared from 3-allyl-4-hydroxy-5-methoxybenzoic acid methyl ester (Example 1, Step 2) by following Method C using methyl iodide as alkylating agent. The reaction was conducted at room temperature for 16 h and crude product was purified by flash column chromatography (96% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07691843B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-ecbe9b079b2447e4a1c9cd9d8e58b046 |
| Source note | uspto-grants-2010_04 |