HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → 4-Allyloxy-3-allylbenzoic acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Methyl 3-allyl-4-hydroxybenzoate | HCID 939882 | — |
| Product | 4-Allyloxy-3-allylbenzoic acid methyl ester | HCID 11241748 | 93% |
Reaction Steps
4-Allyloxy-3-allylbenzoic acid methyl ester was prepared by reacting 3-allyl-4-hydroxybenzoic acid methyl ester (Example 49, Step 2) with allyl bromide following Method C in 93% yield. The reaction was conducted at room temperature for 16 h and the resulting product was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07691843B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-f4c296dd85584bfd8976809853a8fb26 |
| Source note | uspto-grants-2010_04 |