HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 49771646, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 67457354 | HCID 67457354 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | HCID 49771646 | HCID 49771646 | 65.1% |
Reaction Steps
1-Benzyl-4-benzylamino-2-oxo-2,3-dihydro-1H-imidazo[4,5-c]pyridine-6-carboxylic acid methyl ester (0.02 g) was taken up in sulfuric acid (2 mL), and stirred rapidly for 15 mins. The reaction mixture was cooled to 0C, and water was added, which resulted in a precipitate which was filtered and dried in vacuo to give the title compound (10 mg) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07691877B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-0032128e8ef94bd39ad8204d45cdaa7c |
| Source note | uspto-grants-2010_04 |