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HRID639671

反应详情

EQUATION

反应方程式

HRID 639671 的结构方程式

REACTANTS

反应物

4
结构：[I-].[Na+]
HCID5238

Sodium Iodide

INa

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：N#Cc1cccc(CCl)c1
HCID522126

3-(chloromethyl)benzonitrile

C8H6ClN

结构：CCOC(=O)Nc1cc(Br)nc(Br)c1[N+](=O)[O-]
HCID86614481

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)N(Cc1cccc(C#N)c1)c1cc(Br)nc(Br)c1[N+](=O)[O-]
HCID86614488

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

The title compound was prepared following the example in preparation 68 using potassium carbonate (1.50 g), (2,6-dibromo-3-nitro-pyridin-4-yl)-carbamic acid ethyl ester (2.0 g) in acetone (40 ml), 3-chloromethyl-benzonitrile (0.82 g) and sodium iodide (0.98 g). This gave the product (2.62 g) as a yellow oil.