Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Iodide → (3-Cyano-benzyl)-(2,6-dibromo-3-nitro-pyridin-4-yl)-carbamic acid ethyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Iodide | HCID 5238 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 3-(Chloromethyl)benzonitrile | HCID 522126 | — |
| 반응물 | Ethyl (2,6-dibromo-3-nitropyridin-4-yl)carbamate | HCID 86614481 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | (3-Cyano-benzyl)-(2,6-dibromo-3-nitro-pyridin-4-yl)-carbamic acid ethyl ester | HCID 86614488 | — |
반응 단계
The title compound was prepared following the example in preparation 68 using potassium carbonate (1.50 g), (2,6-dibromo-3-nitro-pyridin-4-yl)-carbamic acid ethyl ester (2.0 g) in acetone (40 ml), 3-chloromethyl-benzonitrile (0.82 g) and sodium iodide (0.98 g). This gave the product (2.62 g) as a yellow oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07691877B2 |
| 출처 데이터셋 | uspto-grants-2010_04 |
| ORD ID | ord-1064b08f06124bc7b4e54ddb032fb5d0 |
| 출처 메모 | uspto-grants-2010_04 |