Sodium hydride → HCID 68431774, compound

HRID 639812Notes

Reaction equation

HRID 639812 reaction equation
[I:1][C:2]1[CH:3]=[C:4]([N:8]2[N:12]=[N:11][C:10]([CH2:13][OH:14])=[N:9]2)[CH:5]=[CH:6][CH:7]=1.[H-].[Na+].CS([C:21]1[N:22]([CH3:32])[C:23]([C:26]2[CH:31]=[CH:30][N:29]=[CH:28][CH:27]=2)=[N:24][N:25]=1)(=O)=O>>[I:1][C:2]1[CH:3]=[C:4]([N:8]2[N:12]=[N:11][C:10]([CH2:13][O:14][C:21]3[N:22]([CH3:32])[C:23]([C:26]4[CH:31]=[CH:30][N:29]=[CH:28][CH:27]=4)=[N:24][N:25]=3)=[N:9]2)[CH:5]=[CH:6][CH:7]=1

Participants

4

Reactant 3

HCID 24758Sodium hydrideHCID 221514774-[5-(Methanesulfonyl)-4-methyl-4H-1,2,4-triazol-3-yl]pyridineHCID 68432058HCID 68432058, compound

Product 1

HCID 68431774HCID 68431774, compound

Procedure

The title compound is prepared from [2-(3-iodo-phenyl)-2H-tetrazol-5-yl]-methanol (1 mmol), sodium hydride (1.5 mmol) and 4-(5-methanesulfonyl-4-methyl-4H-[1,2,4]triazol-3-yl)-pyridine (1.25 mmol).

Sources & evidence

ORD record
ord-877e6c5f09e04a31b9b28de7b25a82c6
Source dataset
uspto-grants-2010_04
Patent number
US07691892B2

Reaction notes

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