Sodium hydride → HCID 11596098, compound

HRID 639814Notes

Reaction equation

HRID 639814 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([N:8]2[N:12]=[N:11][C:10]([CH:13]([OH:15])[CH3:14])=[N:9]2)[CH:5]=[CH:6][CH:7]=1.[H-].[Na+].CS([C:22]1[N:23]([CH3:33])[C:24]([C:27]2[CH:28]=[N:29][CH:30]=[CH:31][CH:32]=2)=[N:25][N:26]=1)(=O)=O>>[Cl:1][C:2]1[CH:3]=[C:4]([N:8]2[N:12]=[N:11][C:10]([CH:13]([O:15][C:22]3[N:23]([CH3:33])[C:24]([C:27]4[CH:32]=[CH:31][CH:30]=[N:29][CH:28]=4)=[N:25][N:26]=3)[CH3:14])=[N:9]2)[CH:5]=[CH:6][CH:7]=1

Participants

4

Reactant 3

HCID 24758Sodium hydrideHCID 469283343-[5-(Methanesulfonyl)-4-methyl-4H-1,2,4-triazol-3-yl]pyridineHCID 594242172-(3-chloro-phenyl)-2H-tetrazol-5-yl-ethanol

Product 1

HCID 11596098HCID 11596098, compound

Procedure

The title compound is prepared from 1-[2-(3-chloro-phenyl)-2H-tetrazol-5-yl-ethanol (1 mmol), sodium hydride (1.5 mmol), and 3-(5-methanesulfonyl-4-methyl-4H-[1,2,4]triazol-3-yl)-pyridine (1.25 mmol).

Sources & evidence

ORD record
ord-0be4ca41fe0a480aa38aa9ec9b91c495
Source dataset
uspto-grants-2010_04
Patent number
US07691892B2

Reaction notes

Loading…