HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 11596163, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | HCID 11677501 | HCID 11677501 | — |
| Catalyst | Zinc cyanide (Zn(CN)2) | HCID 11186 | — |
| Product | HCID 11596163 | HCID 11596163 | — |
Reaction Steps
The title compound is prepared from {1-[2-(3-Iodo-phenyl)-2H-tetrazol-5-yl]-ethyl}-methyl-(4-methyl-5-pyridin-4-yl-4H-[1,2,4]triazol-3-yl)-amine (1 mmol), zinc cyanide (1.1 mmol), palladium (0) tetrakis-triphenylphosphine (0.05 mmol) in DMF (5 mL) at 80° C. overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07691892B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-7d7c989f0ecb43639e673ab7b0860321 |
| Source note | uspto-grants-2010_04 |