HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 11589364, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | HCID 11670535 | HCID 11670535 | — |
| Catalyst | Zinc cyanide (Zn(CN)2) | HCID 11186 | — |
| Product | HCID 11589364 | HCID 11589364 | — |
Reaction Steps
The title compound is prepared from 8-[2-(3-iodo-phenyl)-2H-tetrazol-5-ylmethyl]-3-pyridin-4-yl-5,6,7,8-tetrahydro-4H-1,2,3a,8-tetraaza-azulene (1 mmol), zinc cyanide (1.1 mmol), palladium (0) tetrakis-triphenylphosphine (0.05 mmol) in DMF (5 mL) at 80° C. overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07691892B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-c8bd42a8c5434cc9a43b4a49dd77dc13 |
| Source note | uspto-grants-2010_04 |