Triethyl phosphite → HCID 86620235, compound

Participants

Reaction Conditions

Reaction Steps

Triethyl phosphite (0.6 mL) was added to 2-benzyloxy-5-(4-ethylbenzyl)benzylchloride (1.00 g), and the mixture was stirred for 4 hr at 150-160° C. The mixture was purified by silica gel column chromatography (ethyl acetate/n-hexane=1/2) to give the title compound (1.09 g) as a colorless oil.

Provenance & Evidence