Triethyl phosphite → HCID 86620237, compound

Participants

Reaction Conditions

Reaction Steps

Triethyl phosphite (0.8 mL) was added to [5-(4-ethylbenzyl)-2-fluorobenzyl chloride (0.65 g), and the mixture was stirred for 16 hr at 150-160° C. The mixture was purified by silica gel column chromatography (ethyl acetate/n-hexane=1/1) to give the title compound (0.70 g) as a colorless oil.

Provenance & Evidence