HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68422681, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86620240 | HCID 86620240 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68422681 | HCID 68422681 | 94% |
Reaction Steps
To a solution of 2-[5-(4-Ethylbenzyl)-2-hydroxyphenyl]ethylphosphonic acid diethylester (0.50 g) in ethanol (5.0 mL) was added 6N—HCl (5.0 mL), and the reaction mixture was refluxed for 24 hr. Evaporation and crystallization from ethyl acetate-n-hexane gave the title compound (0.40 g) as a colorless crystal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07691898B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-0823b1b1ee1b4127864779ef047d53bf |
| Source note | uspto-grants-2010_04 |