HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59256646, compound → HCID 136352897, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59256646 | HCID 59256646 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 136352897 | HCID 136352897 | 166.7% |
Reaction Steps
A solution of (8-benzyloxy-5,7-dichloro-quinoxalin-2-ylmethyl)dimethylamine (38 mg, 0.105 mmol) in conc HCl (2 mL) was stirred at room temperature for 16 h. The orange solution was concentrated to dryness and the remaining residue was washed with diethyl ether (2 ml×3) to give the desired product as a light yellow solid (27 mg, 83%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07692011B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-05af723e6c1d47d7a22e58b387018a4f |
| Source note | uspto-grants-2010_04 |