HCID 66646129, compound → HCID 11371650, compound

Participants

Reaction Steps

[(R)-3-(3-Chloro-5-fluoro-4-pentyloxy-phenyl)-1-hydroxymethyl-1-methyl-propyl]-carbamic acid tert-butyl ester (10 mg) is dissolved in dioxane containing 4 M HCl (0.5 ml). After stirring at RT for 18 h the product is precipitated by the addition of Et2O to yield the title compound as white solid. MS (ESI+): m/z=319 (MH+).

Provenance & Evidence