HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
7-Methoxyquinoline-8-carboxylic acid → 7-Hydroxyquinoline-8-carboxylic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 7-Methoxyquinoline-8-carboxylic acid | HCID 68774583 | — |
| Lösungsmittel | Hydrogen Bromide | HCID 260 | — |
| Produkt | 7-Hydroxyquinoline-8-carboxylic acid | HCID 135881555 | — |
Reaktionsschritte
The title compound of Step A (2.9 g, 14.1 mmol) in HBr (14 mL) was heated at 90° C. for 1 h. The mixture was then concentrated washed with PhCH3 and used without further purification in subsequent steps.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09447117B2 |
| Quelldatensatz | uspto-grants-2016_09 |
| ORD ID | ord-330dccec023b4fc2842a5a3a605d164e |
| Quellennotiz | uspto-grants-2016_09 |