Piperidine → HCID 11591012, compound

HRID 642194Notes

Reaction equation

HRID 642194 reaction equation
[Li+].[N:2]1([CH2:7][C@@H:8]2[CH2:12][CH2:11][CH2:10][N:9]2[C:13]([C:15]2[CH:31]=[CH:30][C:18]([O:19][CH2:20][C:21]3[CH:29]=[CH:28][C:24]([C:25]([O-])=[O:26])=[CH:23][CH:22]=3)=[CH:17][CH:16]=2)=[O:14])[CH2:6][CH2:5][CH2:4][CH2:3]1.[NH:32]1[CH2:37][CH2:36][CH2:35][CH2:34][CH2:33]1>>[N:32]1([C:25]([C:24]2[CH:28]=[CH:29][C:21]([CH2:20][O:19][C:18]3[CH:17]=[CH:16][C:15]([C:13]([N:9]4[CH2:10][CH2:11][CH2:12][C@H:8]4[CH2:7][N:2]4[CH2:6][CH2:5][CH2:4][CH2:3]4)=[O:14])=[CH:31][CH:30]=3)=[CH:22][CH:23]=2)=[O:26])[CH2:37][CH2:36][CH2:35][CH2:34][CH2:33]1

Participants

3

Reactant 2

HCID 8082PiperidineHCID 23674082HCID 23674082, compound

Product 1

HCID 11591012HCID 11591012, compound

Procedure

The title compound is prepared in a manner substantially analogous to Procedure D from 4-[4-(2-(S)-Pyrrolidin-1-ylmethyl-pyrrolidine-1-carbonyl)-phenoxymethyl]-benzoic acid lithium salt and piperidine. MS (ES+) 476.2

Sources & evidence

ORD record
ord-956fa1cc73334d5dad7ad6ac39fbd3f8
Source dataset
uspto-grants-2010_04
Patent number
US07696234B2

Reaction notes

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