HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68577806, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | HCID 11639561 | HCID 11639561 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 68577806 | HCID 68577806 | — |
Reaction Steps
To a solution of [2-Fluoro-4-(pyridin-2-ylmethoxy)-phenyl]-(2-(S)-pyrrolidin-1-ylmethyl-pyrrolidin-1-yl)-methanone (0.386 g, 1 mmol) in methanol (3 mL) is added a solution of 4M HCl in dioxane (2 mmol). The mixture is concentrated, and the oily residue is dissolved in CH2Cl2 and again concentrated and dried. MS (ES+) 384
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07696234B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-5532e30c5cc64b64aa82ee2373772bf8 |
| Source note | uspto-grants-2010_04 |