HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-methyl-3-pyrrolecarboxylate → HCID 68426167, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-methyl-3-pyrrolecarboxylate | HCID 136747 | — |
| Reactant | Cyclohexane, (bromomethyl)- | HCID 137636 | — |
| Product | HCID 68426167 | HCID 68426167 | — |
Reaction Steps
Prepared from 2-methyl-1H-pyrrole-3-carboxylic acid ethyl ester, example 96(a), and (bromomethyl)cyclohexane under conditions analogous to experimental example 96(b). 1H NMR (200 MHz, CDCl3) δ 6.50 (1H, d, J=3.2 Hz), 6.43 (1H, d, J=3.2 Hz), 4.23 (2H, q, J=7.0 Hz), 3.62 (2H, d, J=6.6 Hz), 2.50 (3H, s), 1.78-0.88 (11H, m), and 1.33 (3H, t, J=7.0 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07696223B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-e736eb5a728e4120a78101737a6485f2 |
| Source note | uspto-grants-2010_04 |