HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N'-Dimethylethylenediamine → HCID 54519504, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N'-Dimethylethylenediamine | HCID 8070 | — |
| Reactant | Iodobenzene | HCID 11575 | — |
| Reactant | Potassium Phosphate, Tribasic | HCID 62657 | — |
| Reactant | Ethyl 3-methyl-1H-indole-2-carboxylate | HCID 593963 | — |
| Catalyst | Copper(1+) iodide; Copper(I) iodide; Cuprous iodide; Cuprous iodide (CuI) | HCID 24350 | — |
| Product | HCID 54519504 | HCID 54519504 | — |
Reaction Steps
Prepared in analogy to that of Example 1(a) from 3-methyl-1H-indole-2-carboxylic acid ethyl ester, iodobenzene, CuI, N,N′-dimethylethylenediamine, and potassium phosphate. 1H NMR (200 MHz, CDCl3): δ (ppm)=7.7-7.0 (m, 9H), 4.15 (q, 2H, J=7.1 Hz), 2.67 (s, 3H), 1.10 (t, 3H, J=7.1 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07696223B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-a9cea89df42e49af95b547fe026416cb |
| Source note | uspto-grants-2010_04 |