HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(Bromomethyl)naphthalene → HCID 58900227, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(Bromomethyl)naphthalene | HCID 137844 | — |
| Reactant | HCID 68579658 | HCID 68579658 | — |
| Product | HCID 58900227 | HCID 58900227 | — |
Reaction Steps
3-(3-Carboxy-propyl)-1H-indole-2-carboxylic acid (Lit. 3) was esterified using HCl/MeOH to give the 3-(3-methoxycarbonyl-propyl)-1H-indole-2-carboxylic acid methyl ester. Using general procedure B, 3-(3-methoxycarbonyl-propyl)-1H-indole-2-carboxylic acid methyl ester was coupled with 1-bromomethyl-naphthalene and the product obtained was hydrolyzed to give the title compound as a white solid. MS: 386.3 ([M−H]−).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07696240B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-c40c7bfa10924128a10c33a4de17c6b5 |
| Source note | uspto-grants-2010_04 |