HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylsilane → HCID 68577977, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylsilane | HCID 12052 | — |
| Reactant | HCID 68578556 | HCID 68578556 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 68577977 | HCID 68577977 | — |
Reaction Steps
2. To a solution of 3-(naphthalene-1-carbonyl)-1H-indole-2-carboxylic acid ethyl ester (0.81 g) in trifluoroacetic acid (3.6 ml) was added triethylsilane (1.5 ml) and stirring was continued at 22° C. for 21 h. The suspension was filtered, the residue washed with n-heptane and dried to give 3-naphthalen-1-ylmethyl-1H-indole-2-carboxylic acid ethyl ester as a white solid. MS: 328.1 ([M−H]−).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07696240B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-9cdc923ef8c94c118addd54d147844e9 |
| Source note | uspto-grants-2010_04 |