HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyldimethylsilyl chloride → HCID 59676079, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyldimethylsilyl chloride | HCID 28928 | — |
| Reactant | HCID 59676100 | HCID 59676100 | — |
| Product | HCID 59676079 | HCID 59676079 | — |
Reaction Steps
Following the procedure described in Example 80, using 6,7-Dihydro-12H-5-thia-12-aza-dibenzo[a,e]azulen-9-ol (350 mg, 1.31 mmol) and TBSCl (225 mg, 1.50 mmol) as the starting material, the title compound was prepared as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07696239B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-e65b785ba8d04a9ba9c5e0100d9c9967 |
| Source note | uspto-grants-2010_04 |