Methanol → HCID 24988738, compound

Participants

Reaction Steps

To a solution of Example 48 in a 2:1 mixture of methanol and water was added 1.0 equivalent of oxone. The mixture was stirred at room temperature for 10 min and directly subjected to reverse phase HPLC to isolate the title compound as a white powder after lyophilization. MS found for C22H20ClN5O4S2 (M+H)+ 518.1, 520.1 (Cl pattern).

Provenance & Evidence