Methanol → HCID 24988739, compound

Participants

Reaction Steps

To a solution of Example 48 in a 2:1 mixture of methanol and water was added 3 equivalent of oxone. The mixture was stirred at room temperature for 1 hr and directly subjected to reverse phase HPLC to isolate the title compound as a white powder after lyophilization. MS found for C22H20ClN5O5S2 (M+H)+ 534.1, 536.1 (Cl pattern).

Provenance & Evidence