HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 643062Generated: October 31, 2026
Hydrochloric Acid → HCID 123608631, compound
https://huagongshe.com/reaction/643062
Participants
| Role | Name | HCID | Charge |
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| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 68294422 | HCID 68294422 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 123608631 | HCID 123608631 | 100% |
Reaction Steps
A solution of Example 5F in THF (4 mL) was treated with 4N HCl, and stirred at 70° C. for 3 hrs. The mixture was cooled to room temperature and quenched with saturated sodium bicarbonate and ethyl acetate. The organic layer was separated, washed with brine, dried over sodium sulfate, filtered and the solvents were evaporated to give 83 mg (100%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07696226B2 |
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| Source dataset | uspto-grants-2010_04 |
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| ORD ID | ord-51d6f924452e41ac81a0ec95cfce4330 |
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| Source note | uspto-grants-2010_04 |
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