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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 643062Generated: October 31, 2026

Hydrochloric Acid → HCID 123608631, compound

https://huagongshe.com/reaction/643062

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 68294422HCID 68294422—
SolventTetrahydrofuranHCID 8028—
ProductHCID 123608631HCID 123608631100%

Reaction Conditions

Temperature70 °C

Reaction Steps

A solution of Example 5F in THF (4 mL) was treated with 4N HCl, and stirred at 70° C. for 3 hrs. The mixture was cooled to room temperature and quenched with saturated sodium bicarbonate and ethyl acetate. The organic layer was separated, washed with brine, dried over sodium sulfate, filtered and the solvents were evaporated to give 83 mg (100%) of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07696226B2
Source datasetuspto-grants-2010_04
ORD IDord-51d6f924452e41ac81a0ec95cfce4330
Source noteuspto-grants-2010_04