HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68580868, compound → HCID 15981170, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68580868 | HCID 68580868 | — |
| Solvent | Formic Acid | HCID 284 | — |
| Product | HCID 15981170 | HCID 15981170 | — |
Reaction Steps
A solution of [3′-(4-cyano-[1,3,5]triazin-2-ylamino) -biphenyl-4-ylmethyl]-carbamic acid tert-butyl ester (43 mg) in formic acid (1 ml) is stirred at 5° C. for 4.5 h. This solution is evaporated under reduced pressure. The remaining oil is treated with diethyl ether to obtain crystals of 4-(4′-aminomethyl-biphenyl-3-ylamino)-[1,3,5]triazine-2-carbonitrile, salt with formic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07700605B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-ad91e6c3920a45c1bc34c44a481f3bbc |
| Source note | uspto-grants-2010_04 |