HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59261072, compound → HCID 59261064, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59261072 | HCID 59261072 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 59261064 | HCID 59261064 | — |
Reaction Steps
1-[3-(Acetyloxy)-1-({[2-tert-butoxy-5-(trifluoromethyl)benzyl]amino}carbonyl)cyclopentyl]ethyl acetate (7.0 g, 14.4 mmol) was dissolved in anhydrous 4N HCl in dioxane (40 mL) and stirred at rt for 65 min. The reaction mixture was then concentrated to give 3-[1-(acetyloxy)ethyl]-3-({[2-hydroxy-5-(trifluoromethyl)benzyl]amino}carbonyl)cyclopentyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07700591B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-8b92dcb888594c7cbe6b350b77e05a95 |
| Source note | uspto-grants-2010_04 |