Hydrochloric Acid → HCID 86604120, compound

Participants

Reaction Steps

tert-Butyl 4-(3-{[(4-methylphenyl)sulfonyl]oxy}isoxazol-5-yl)piperidine-1-carboxylate (719 mg, 1.76 mmol) was dissolved in anhydrous 4N HCl in dioxane (15 mL) and the resulting solution was stirred at rt for 1 h. The reaction mixture was concentrated to afford 5-piperidin-4-ylisoxazol-3-yl 4-methylbenzenesulfonate hydrochloride, which did not require further purification.

Provenance & Evidence