HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methane → HCID 11408320, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | L-Tartaric acid | HCID 444305 | — |
| Reactant | HCID 11408320 | HCID 11408320 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 11408320 | HCID 11408320 | — |
| Product | HCID 67481247 | HCID 67481247 | — |
Reaction Steps
To a heated solution of (1R,2R,3S,5S)-2-methoxymethyl-3-(3,4-dichlorophenyl)-8-azabicyclo[3.2.1]octane (the free base) in aqueous ethanol was added L-tartaric acid. The warm mixture was treated with activated charcoal and filtered. The filtrate was cooled and (1R,2R,3S,5S)-2-methoxymethyl-3-(3,4-dichlorophenyl)-8-azabicyclo-[3.2.1]octane was isolated as the L-tartrate monohydrate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07700619B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-660a47fde6dc4b599968f2185b786729 |
| Source note | uspto-grants-2010_04 |