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HRID643759

反应详情

EQUATION

反应方程式

HRID 643759 的结构方程式

REACTANTS

反应物

2
结构：CN(C)C=C1CCc2nonc2C1=O
HCID67405521

未命名化合物

结构：N=C(N)Nc1cccc(O)c1
HCID178418735

未命名化合物

PRODUCTS

生成物

1
结构：Oc1cccc(Nc2ncc3c(n2)-c2nonc2CC3)c1
HCID11403271

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

The DMF solution of 5-dimethylaminomethylene-6,7-dihydro-5H-benzo[1,2,5]oxadiazol-4-one 0.1 g (0.00052 mol) and 3 equivalents of N-(3-hydroxy-phenyl)-guanidine was stirred at 110° C. for overnight, the final product was purified by directly injecting the DMF reaction solution into prep HPLC.

WORKUP

后处理

  1. customthe final product was purified
  2. customthe DMF reaction solution into prep HPLC