huagongshe.com
HRID643762

反应详情

EQUATION

反应方程式

HRID 643762 的结构方程式

REACTANTS

反应物

3
结构：CN(C)C=O
HCID6228

N,N-Dimethylformamide

C3H7NO

结构：CN(C)C=C1CCc2ccccc2C1=O
HCID54406509

2-[(Dimethylamino)methylene]-3,4-dihydro-1(2H)-naphthalenone

C13H15NO

结构：N=C(N)Nc1ccccc1
HCID178418923

未命名化合物

PRODUCTS

生成物

1
结构：c1ccc(Nc2ncc3c(n2)-c2ccccc2CC3)cc1
HCID67406319

未命名化合物

PROCEDURE

实验过程

A solution of 2-dimethylaminomethylene-3,4-dihydro-2H-naphthalen-1-one 100 mg in 5 ml DMF and 3 eq. of N-phenyl-guanidine was stirred at 110° C. for overnight, the product was purified by directly injecting the DMF reaction solution into prep HPLC.

WORKUP

后处理

  1. customthe product was purified
  2. customthe DMF reaction solution into prep HPLC