HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4-Phenylphenol → 5-(3-Chloro-biphenyl-4-yloxymethyl)-furan-2-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4-Phenylphenol | HCID 7074 | — |
| Reactant | Methyl 5-(chloromethyl)-2-furoate | HCID 75065 | — |
| Product | 5-(3-Chloro-biphenyl-4-yloxymethyl)-furan-2-carboxylic acid | HCID 11221165 | — |
Reaction Steps
5-(3-Chloro-biphenyl-4-yloxymethyl)-furan-2-carboxylic acid was prepared using general procedure A from 2-chloro-4-phenylphenol (available from TCI America, Portland, Oreg.) and 5-chloromethylfuran-2-carboxylic acid methyl ester (available from Aldrich, Milwaukee, Wis., or from Maybridge plc, Tintagel, UK). Yield: 66 mg. Mass spectrum (ES) MH+=329.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07700632B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-12f4a147e2ac42bd99d7f4543aac34a9 |
| Source note | uspto-grants-2010_04 |