4-Hydroxybiphenyl → HCID 11403945, compound

HRID 643801Notes

Reaction equation

HRID 643801 reaction equation
[C:1]1([C:7]2[CH:12]=[CH:11][C:10]([OH:13])=[CH:9][CH:8]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C[O:15][C:16](=[O:25])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=1[CH2:23]Br>>[C:7]1([C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)[CH:8]=[CH:9][C:10]([O:13][CH2:23][C:18]2[CH:19]=[CH:20][CH:21]=[CH:22][C:17]=2[C:16]([OH:25])=[O:15])=[CH:11][CH:12]=1

Participants

3

Reactant 2

HCID 71034-HydroxybiphenylHCID 2734813Methyl 2-(bromomethyl)benzoate2×

Product 1

HCID 11403945HCID 11403945, compound

Procedure

2-(Biphenyl-4-yloxymethyl)-benzoic acid was prepared using general procedure A from 4-phenylphenol (available from Aldrich, Milwaukee, Wis.) and 2-bromomethyl-benzoic acid methyl ester (Intermediate 1). Yield: 50 mg. Mass spectrum (ES) MH+=305.

Sources & evidence

ORD record
ord-8b8ba508616845bc845ccb2963490e4b
Source dataset
uspto-grants-2010_04
Patent number
US07700632B2

Reaction notes

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