Trifluoroacetic acid → HCID 66750557, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of {3-[6-benzyloxy-7-(1,1,4-trioxo-1,2,5-thiadiazolidin-2-yl)-naphthalen-2-yl]-phenyl}-acetic acid (600 mg, 1.2 mmol) in EtOH (50 mL) is added TFA (25 mL) and the mixture is heated at 40° C. for 2 h. EtOH and TFA are removed via vacuum and the residue is purified by HPLC to give the title compound.

Provenance & Evidence