Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 643892Generated: October 30, 2026

HCID 66750641, compound → HCID 59263256, compound

https://huagongshe.com/reaction/643892

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 66750641HCID 66750641—
SolventMethanolHCID 887—
ProductHCID 59263256HCID 59263256—

Reaction Steps

The title compound is prepared analogously to Example 32, step B, starting from 5-[6-hydroxy-7-(1,1,4-trioxo-1,2,5-thiadiazolidin-2-yl)-naphthalen-2-yl]-2-methylpentanoic acid ethyl ester (Example 9-4) and the reaction is performed in solvent MeOH instead of i-PrOH: Retention time=1.17 min (Method A); (M−H)−=405.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07700633B2
Source datasetuspto-grants-2010_04
ORD IDord-fc2b922691194798867b7060ad2fd12e
Source noteuspto-grants-2010_04