HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66750641, compound → HCID 59263256, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66750641 | HCID 66750641 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59263256 | HCID 59263256 | — |
Reaction Steps
The title compound is prepared analogously to Example 32, step B, starting from 5-[6-hydroxy-7-(1,1,4-trioxo-1,2,5-thiadiazolidin-2-yl)-naphthalen-2-yl]-2-methylpentanoic acid ethyl ester (Example 9-4) and the reaction is performed in solvent MeOH instead of i-PrOH: Retention time=1.17 min (Method A); (M−H)−=405.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07700633B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-fc2b922691194798867b7060ad2fd12e |
| Source note | uspto-grants-2010_04 |