HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66750744, compound → HCID 66750617, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66750744 | HCID 66750744 | — |
| Catalyst | Platinum | HCID 23939 | — |
| Product | HCID 66750617 | HCID 66750617 | — |
Reaction Steps
To a solution of 6-benzyloxy-2-ethyl-7-nitro-1,2,3,4-tetrahydronaphthalene (490 mg, 1.57 mmol) is added 5% Pt/C (680 mg) and stirred under hydrogen atmosphere (1 atm) for 18 h. It is then filtered through Celite and the filtrate is concentrated. The residue is purified by column chromatography to give the title compound as a brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07700633B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-987ea5962c44468b82c8ecf8cb185750 |
| Source note | uspto-grants-2010_04 |